33-0991
KHF2*0.8NH4HF2
Triklin
Dexp Dcal d(D) h k l
7.0600 7.0499 .0101 0 1 0
4.0800 4.0813 -.0013 0 -1 2
3.6200 3.6205 -.0005 1 -2 1
3.5000 3.4998 .0002 0 -2 2
2.8900 2.8908 -.0008 -1 1 2
2.8300 2.8281 .0019 -2 0 2
2.7000 2.7022 -.0022 1 0 2
2.6400 2.6400 .0000 0 -3 2
2.5900 2.5863 .0037 -1 -2 3
2.5300 2.5275 .0025 2 1 0
2.3800 2.3768 .0032 0 0 3
2.2600 2.2592 .0008 -1 -3 1
A= 6.532 DA= .005
B= 8.181 DB= .002
C= 8.389 DC= .004
GAMMA= 99.35 DGAMMA= .05
BETA =103.3074 DBETA = .0002
ALPHA=115.499 DALPHA= .001
V=376.1
33-0992
KSb2F7
Triklin
Dexp Dcal d(D) h k l
10.2000 10.2009 -.0009 1 0 0
6.0800 6.0824 -.0024 0 1 1
5.1300 5.1315 -.0015 -2 -1 1
4.6900 4.6898 .0002 -1 0 2
4.2500 4.2505 -.0005 -2 -1 2
3.7800 3.7765 .0035 -2 -2 2
3.6800 3.6771 .0029 0 -3 1
3.6000 3.6012 -.0012 -2 1 2
3.3500 3.3498 .0002 -3 0 2
3.3000 3.2980 .0020 2 -2 1
3.1300 3.1314 -.0014 -2 -3 2
3.6300 3.6320 -.0020 1 2 1
A= 11.04563 DA= .00009
B= 11.247 DB= .002
C= 9.7725 DC= .0003
GAMMA= 83.76 DGAMMA= .01
BETA =112.560 DBETA = .006
ALPHA=105.93 DALPHA= .01
V= 1078.2
33-0997
K2Bi4S7
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
3.9200 3.9200 .0000 -1 1 1
3.7700 3.7719 -.0019 1 1 1
3.4900 3.4913 -.0013 1 1 2
3.4300 3.4277 .0023 -3 0 2
3.2300 3.2287 .0013 -2 1 2
3.1100 3.1068 .0032 0 1 4
2.9300 2.9316 -.0016 3 0 2
2.8400 2.8415 -.0015 1 1 4
2.6300 2.6319 -.0019 -2 1 5
2.2600 2.2595 .0005 -1 1 7
2.0900 2.0896 .0004 1 2 0
2.0200 2.0194 .0006 3 0 6
1.9450 1.9452 -.0002 1 2 3
1.6130 1.6127 .0003 4 1 6
a= 10.3800 b= 4.2720 c= 18.64000 beta= 103.744
da= .0007 db=.005 dc= .00006 dbet=.004
V= 802.8
33-0998
KBi3S5
Triklin
Dexp Dcal d(D) h k l
3.7700 3.7682 .0018 -2 1 1
3.6900 3.6898 .0002 2 0 0
3.4900 3.4924 -.0024 -1 -3 1
3.4100 3.4109 -.0009 -2 0 2
3.3100 3.3083 .0017 -2 2 1
3.2400 3.2406 -.0006 -2 1 2
3.1200 3.1230 -.0030 0 2 2
3.0200 3.0192 .0008 -1 -3 2
2.9700 2.9699 .0001 0 4 0
2.8400 2.8396 .0004 -1 0 3
2.8000 2.7979 .0021 2 1 1
2.7400 2.7416 -.0016 2 -2 1
A= 7.9667 DA= .0008
B= 11.964 DB= .001
C= 8.565 DC= .002
GAMMA= 91.10 DGAMMA= .02
BETA =111.870 DBETA = .001
ALPHA= 95.84 DALPHA= .02
V=752.4
33-1000
K3B12BrH12
Monoklin
Grupa 4, 11
Dexp Dcal d(D) h k l
6.8400 6.8323 .0077 1 1 0
5.0200 5.0257 -.0057 1 0 2
4.6900 4.6908 -.0008 2 1 1
3.4400 3.4358 .0042 -1 1 2
3.1800 3.1798 .0002 2 2 2
2.9320 2.9288 .0032 0 1 3
2.6120 2.6119 .0001 4 1 2
2.4490 2.4488 .0002 4 1 0
2.4240 2.4246 -.0006 2 1 4
2.3660 2.3664 -.0004 -1 3 2
2.2720 2.2722 -.0002 -2 0 3
1.7650 1.7650 .0000 4 4 1
1.6000 1.5998 .0002 1 1 6
a= 11.047 b= 9.232 c= 10.0750 beta= 66.862
da=.001 db=.001 dc=.0005 dbet= .007
V= 944.9
33-1047
K5Tl{SeO4}4
Triklin
Dexp Dcal d(D) h k l
9.9000 9.8946 .0054 -1 0 1
7.7800 7.7724 .0076 1 1 0
6.0700 6.0720 -.0020 -1 -1 2
5.8500 5.8538 -.0038 -1 1 1
5.2600 5.2553 .0047 2 1 0
4.6300 4.6290 .0010 0 2 0
4.4600 4.4586 .0014 0 1 2
4.1400 4.1408 -.0008 -2 -2 2
4.0900 4.0892 .0008 -3 -1 1
3.8580 3.8597 -.0017 -2 1 2
3.7610 3.7628 -.0018 3 1 0
3.5880 3.5870 .0010 1 -2 2
A= 12.5514 DA= .0005
B= 9.859 DB= .003
C= 12.996 DC= .001
GAMMA= 76.592 DGAMMA= .006
BETA =110.67 DBETA = .01
ALPHA=108.635 DALPHA= .008
V= 1413.0
33-1835
C6H18O3S3*KC48
Triklin
Dexp Dcal d(D) h k l
4.9800 4.9733 .0067 1 0 1
4.0800 4.0813 -.0013 2 -1 1
3.6200 3.6174 .0026 0 1 1
3.1600 3.1560 .0040 -1 -2 1
2.8000 2.8003 -.0003 -2 1 1
2.5000 2.4963 .0037 0 -3 1
2.1100 2.1096 .0004 -2 0 2
1.7900 1.7900 -.0000 0 4 0
1.6700 1.6701 -.0001 6 -2 1
1.5500 1.5500 .0000 2 1 3
1.1400 1.1400 -.0000 6 -4 4
1.0900 1.0900 -.0000 -4 -2 4
A= 10.619 DA= .005
B= 7.6277 DB= .0004
C= 5.514 DC= .001
GAMMA= 96.70 DGAMMA= .08
BETA = 76.58 DBETA = .03
ALPHA=110.04 DALPHA= .02
V= 407.8
33-1836
C6H18O3S3*KC24
Monoklin
Grupa 4, 11
Dexp Dcal d(D) h k l
4.6100 4.6104 -.0004 1 1 0
3.6800 3.6784 .0016 0 0 1
3.0800 3.0817 -.0017 3 0 0
2.6500 2.6479 .0021 -2 0 1
2.0400 2.0405 -.0005 2 2 1
1.8300 1.8301 -.0001 2 0 2
1.6700 1.6698 .0002 4 2 1
1.5400 1.5401 -.0001 -2 1 2
1.2200 1.2200 -.0000 3 0 3
1.1500 1.1500 .0000 4 1 3
1.0800 1.0803 -.0003 7 2 2
a= 9.410 b= 5.3190 c= 3.7440 beta= 79.253
da= .001 db= .0001 dc= .0001 dbet= .003
V= 184.1
33-1837
C3H2Cl2KN5O*2H2O
Monoklin
Grupa 4, 11
Dexp Dcal d(D) h k l
10.0000 10.0538 -.0538 0 0 1
7.2720 7.2495 .0225 0 1 1
4.6380 4.6408 -.0028 0 2 1
3.3460 3.3513 -.0053 0 0 3
3.2920 3.2950 -.0030 0 3 1
3.1460 3.1449 .0011 -1 0 1
3.0150 3.0118 .0032 -1 1 1
2.9860 2.9944 -.0084 1 1 2
2.8660 2.8655 .0005 0 3 2
2.6500 2.6501 -.0001 1 0 3
2.5130 2.5135 -.0005 0 0 4
2.3780 2.3783 -.0003 -1 2 2
a= 3.5470 b= 10.463 c= 10.196 beta= 80.413
da=.0001 db=.001 dc=.001 dbet=.002
V= 373.1
33-1838
C3H3Cl2KN6
Triklin
Dexp Dcal d(D) h k l
9.6000 9.5943 .0057 1 0 0
5.0120 5.0236 -.0116 1 1 1
4.1870 4.1833 .0037 0 1 2
4.0920 4.0901 .0019 1 0 2
4.0190 4.0198 -.0008 -2 0 1
3.7420 3.7453 -.0033 1 1 2
3.5840 3.5811 .0029 2 1 1
3.4870 3.4880 -.0010 0 -1 2
3.3830 3.3825 .0005 2 0 2
3.2970 3.2969 .0001 0 2 2
3.2500 3.2498 .0002 2 -2 1
3.1440 3.1447 -.0007 3 -1 1
A= 10.115 DA= .001
B= 8.544 DB= .006
C= 8.8285 DC= .0005
GAMMA=107.54 DGAMMA= .06
BETA = 87.84 DBETA = .01
ALPHA= 78.86 DALPHA= .02
V=708.7
33-1839
C6H7KO2
Triklin
Dexp Dcal d(D) h k l
16.4500 16.4689 -.0189 0 0 1
8.1800 8.1854 -.0054 -1 0 1
5.5900 5.5979 -.0079 2 0 1
5.4400 5.4392 .0008 2 0 0
4.4000 4.3987 .0013 0 2 2
4.0800 4.0770 .0030 -1 1 3
3.7700 3.7665 .0035 2 0 4
3.7100 3.7076 .0024 -2 -2 1
3.6200 3.6166 .0034 3 1 3
3.4800 3.4814 -.0014 2 2 4
3.2600 3.2605 -.0005 1 3 0
3.1400 3.1406 -.0006 -2 2 1
A= 11.694 DA= .004
B= 10.021 DB= .001
C= 17.390 DC= .004
GAMMA= 73.89 DGAMMA= .01
BETA = 72.99 DBETA = .01
ALPHA= 77.97 DALPHA= .03
V=1854.4