21-0317
DyK{SO4}2*H2O
Triklin
Dexp Dcal d(D) h k l
5.9800 5.9776 .0024 1 0 0
3.7300 3.7319 -.0019 0 1 2
3.3600 3.3566 .0034 0 2 0
3.2400 3.2375 .0025 1 -1 1
3.1200 3.1195 .0005 2 1 0
3.0600 3.0595 .0005 -2 0 1
2.7520 2.7554 -.0034 -2 -1 2
2.6090 2.6113 -.0023 2 0 1
2.5650 2.5634 .0016 -1 -1 3
2.4380 2.4380 -.0000 -1 2 2
2.2080 2.2086 -.0006 2 -1 1
2.1190 2.1191 -.0001 -1 2 3
A= 6.4496 DA= .0003
B= 7.0854 DB= .0004
C= 8.4931 DC= .0001
GAMMA= 72.917 DGAMMA= .001
BETA =102.468 DBETA = .001
ALPHA= 86.567 DALPHA= .001
V=359.1
21-00322
ErK{SO4}2*1.75H2O
Triklin
Dexp Dcal d(D) h k l
6.0900 6.0927 -.0027 0 1 1
4.2600 4.2566 .0034 -1 -2 1
3.9500 3.9521 -.0021 0 -2 2
3.8700 3.8728 -.0028 1 1 2
3.7200 3.7200 .0000 1 -2 1
3.4300 3.4342 -.0042 0 -3 1
3.3600 3.3596 .0004 1 3 0
3.1500 3.1538 -.0038 2 2 0
3.0800 3.0799 .0001 1 -1 3
3.0300 3.0318 -.0018 1 3 1
2.8330 2.8313 .0017 1 -3 1
2.7340 2.7307 .0033 2 3 0
A= 6.9107 DA= .0001
B= 10.6207 DB= .0001
C= 9.80057 DC= .00008
GAMMA= 77.310 DGAMMA= .002
BETA = 79.651 DBETA = .001
ALPHA=101.862 DALPHA= .002
V=667.5
21-0380
H6K4{PO4}2P2O7
Triklin
Dexp Dcal d(D) h k l
7.7300 7.7231 .0069 0 1 1
6.2200 6.2097 .0103 0 -1 1
6.0400 6.0462 -.0062 1 0 1
4.7100 4.7096 .0004 1 2 1
4.5800 4.5803 -.0003 1 -2 1
4.2900 4.2897 .0003 -1 0 1
4.2100 4.2138 -.0038 -1 2 1
3.9800 3.9788 .0012 1 1 2
3.5600 3.5608 -.0008 1 3 0
3.5300 3.5290 .0010 0 -1 2
3.5000 3.4992 .0008 0 3 2
3.3300 3.3258 .0042 -1 -2 1
A= 6.857 DA= .004
B= 15.095 DB= .004
C= 8.43 DC= .01
GAMMA= 96.10 DGAMMA= .08
BETA = 72.29 DBETA = .04
ALPHA= 77.76 DALPHA= .08
V= 798.9
21-0382
K8H2P4O15
Triklin
Dexp Dcal d(D) h k l
4.6400 4.6384 .0016 -1 1 1
4.4400 4.4400 .0000 -1 -1 1
3.9800 3.9808 -.0008 1 1 2
3.0700 3.0684 .0016 -1 2 0
3.0300 3.0290 .0010 0 -2 1
2.9280 2.9275 .0005 0 1 3
2.8580 2.8575 .0005 -1 2 2
2.7850 2.7863 -.0013 0 0 3
2.7280 2.7267 .0013 -2 1 2
2.6410 2.6445 -.0035 -2 -1 2
2.5750 2.5765 -.0015 0 3 1
2.4960 2.4950 .0010 -3 -1 1
A= 8.2207 DA= .0002
B= 7.9828 DB= .0001
C= 8.83112 DC= .00001
GAMMA= 75.589 DGAMMA= .001
BETA = 85.470 DBETA = .001
ALPHA= 71.182 DALPHA= .001
V=531.3
21-0383
K2H8P4O15
Triklin
Dexp Dcal d(D) h k l
7.4500 7.4282 .0218 0 1 1
6.0600 6.0650 -.0050 2 0 0
5.9200 5.9124 .0076 0 -1 1
5.0100 5.0088 .0012 2 -1 1
4.8800 4.8817 -.0017 -2 1 1
4.6800 4.6948 -.0148 2 1 0
4.5500 4.5502 -.0002 -2 0 1
4.3500 4.3555 -.0055 -2 2 1
4.0800 4.0898 -.0098 1 0 2
3.8800 3.8800 -.0000 -3 2 0
3.8000 3.8005 -.0005 -1 3 0
3.6700 3.6694 .0006 -3 1 1
A= 12.8385 DA= .0001
B= 11.62850 DB= .00003
C= 8.48096 DC= .00009
GAMMA=106.9405 DGAMMA= .0004
BETA = 84.83862 DBETA = .00004
ALPHA= 78.7217 DALPHA= .0003
V=1173.1
21-0384
H3KP2O7*H2O
Triklin
Dexp Dcal d(D) h k l
8.7500 8.7144 .0356 2 0 0
7.0700 7.0772 -.0072 0 1 0
6.4000 6.4005 -.0005 1 1 1
5.6900 5.6740 .0160 2 1 1
5.2100 5.2049 .0051 0 -1 1
4.9200 4.9240 -.0040 1 -1 1
4.4700 4.4699 .0001 0 1 2
4.2700 4.2804 -.0104 2 1 2
4.1100 4.1183 -.0083 4 0 1
3.8400 3.8430 -.0030 -4 0 1
3.7300 3.7305 -.0005 -2 1 2
3.6300 3.6300 -.0000 1 2 1
A= 17.7194 DA= .0003
B= 7.3367 DB= .0005
C= 9.9944 DC= .0005
GAMMA= 81.050 DGAMMA= .005
BETA = 82.85 DBETA = .01
ALPHA= 76.681 DALPHA= .006
V=1243.6
21-0385
H2K2P2O7*.5H2O
Triklin
Dexp Dcal d(D) h k l
7.6800 7.6707 .0093 0 0 1
6.3300 6.3392 -.0092 -1 1 0
6.1000 6.1007 -.0007 0 -2 1
5.2000 5.2008 -.0008 0 -3 1
4.9500 4.9639 -.0139 -1 3 0
4.5200 4.5249 -.0049 1 -2 1
4.4500 4.4492 .0008 0 -4 1
4.3600 4.3611 -.0011 0 5 1
4.1300 4.1367 -.0067 -1 -3 1
3.8500 3.8488 .0012 0 -5 1
3.8100 3.8098 .0002 0 2 2
3.5200 3.5171 .0029 0 -2 2
A= 6.747 DA= .003
B= 24.42 DB= .01
C= 7.762 DC= .004
GAMMA= 85.05 DGAMMA= .03
BETA = 86.16 DBETA = .03
ALPHA= 81.79 DALPHA= .01
V= 1259.3
21-0386
HK3P2O7*3H2O
Triklin
Dexp Dcal d(D) h k l
8.4500 8.4587 -.0087 1 2 0
6.5200 6.5203 -.0003 1 1 1
5.2400 5.2424 -.0024 3 2 0
5.1400 5.1371 .0029 3 0 0
4.9900 4.9920 -.0020 0 2 1
4.9200 4.9148 .0052 -1 -3 1
4.4600 4.4632 -.0032 -3 1 0
4.2300 4.2294 .0006 2 4 0
3.9400 3.9425 -.0025 -3 -3 1
3.8300 3.8292 .0008 4 3 0
3.5700 3.5693 .0007 -1 3 1
3.4800 3.4801 -.0001 0 1 2
A= 16.563 DA= .006
B= 17.405 DB= .005
C= 7.66275 DC= .00007
GAMMA= 70.98 DGAMMA= .05
BETA = 83.35 DBETA = .01
ALPHA= 98.75 DALPHA= .01
V=2030.3
21-0619
KNH4{PO3F}
Triklin
Dexp Dcal d(D) h k l
6.5000 6.5014 -.0014 0 1 1
5.2000 5.2027 -.0027 0 -1 1
4.4500 4.4509 -.0009 1 1 0
4.3500 4.3524 -.0024 2 0 1
4.1700 4.1679 .0021 1 1 2
3.9700 3.9706 -.0006 -1 1 2
3.3000 3.3003 -.0003 2 -2 1
3.2700 3.2698 .0002 2 0 3
3.1600 3.1595 .0005 2 1 2
3.0700 3.0688 .0012 0 -2 1
2.9900 2.9894 .0006 -2 1 2
2.9500 2.9491 .0009 1 2 1
2.9000 2.9005 -.0005 -1 -1 2
2.8700 2.8711 -.0011 1 2 2
A= 9.309 DA= .005
B= 7.6153 DB= .0008
C= 11.110 DC= .003
GAMMA=110.68 DGAMMA= .04
BETA = 72.52 DBETA = .01
ALPHA= 83.97 DALPHA= .01
V= 682.9
21-0620
Gamma-KBa2{OH}9
Triklin
Dexp Dcal d(D) h k l
3.6600 3.6604 -.0004 0 1 1
3.4700 3.4716 -.0016 2 -2 0
3.3800 3.3798 .0002 1 -1 1
3.2700 3.2744 -.0044 0 4 0
2.6400 2.6402 -.0002 1 3 1
2.5600 2.5598 .0002 -2 4 0
2.5500 2.5493 .0007 2 4 0
2.4400 2.4396 .0004 1 -4 1
2.2700 2.2700 .0000 -3 0 1
2.2300 2.2301 -.0001 0 -5 1
2.0400 2.0417 -.0017 4 0 0
1.9500 1.9501 -.0001 0 -6 1
A= 8.173 DA= .002
B= 13.1191 DB= .0002
C= 3.8853 DC= .0009
GAMMA= 90.120 DGAMMA= .007
BETA = 92.24 DBETA = .07
ALPHA= 93.263 DALPHA= .004
V=415.3
21-0621
K2BiCl5
Triklin
Dexp Dcal d(D) h k l
6.7600 6.7458 .0142 0 0 1
6.2000 6.1957 .0043 1 0 0
4.3300 4.3305 -.0005 0 -2 1
4.0200 4.0193 .0007 0 2 0
3.6900 3.6883 .0017 -1 -2 1
3.6000 3.5990 .0010 1 -1 2
3.5100 3.5105 -.0005 1 0 2
3.1300 3.1333 -.0033 2 1 1
2.9450 2.9434 .0016 0 -3 1
2.8690 2.8681 .0009 2 2 0
2.7340 2.7350 -.0010 2 -1 2
2.6530 2.6542 -.0012 -2 1 0
A= 6.679 DA= .002
B= 8.944 DB= .001
C= 7.677 DC= .001
GAMMA= 80.90 DGAMMA= .02
BETA = 74.90 DBETA = .01
ALPHA=110.72 DALPHA= .06
V= 397.9
21-0622
K2B8O13
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2959 .0041 0 1 1
5.7800 5.7769 .0031 0 -1 1
4.6500 4.6524 -.0024 -1 -1 1
3.6900 3.6902 -.0002 -1 -3 1
3.3800 3.3816 -.0016 2 2 0
3.3000 3.3001 -.0001 -2 1 0
3.1000 3.0979 .0021 -2 -1 1
2.9000 2.9002 -.0002 -1 -1 2
2.8600 2.8599 .0001 -1 2 2
2.7800 2.7796 .0004 1 6 0
2.7400 2.7404 -.0004 0 6 1
2.7000 2.7010 -.0010 -1 3 2
A= 6.997 DA= .004
B= 17.411 DB= .003
C= 6.4900 DC= .0006
GAMMA= 82.00 DGAMMA= .02
BETA = 91.77 DBETA = .02
ALPHA= 82.849 DALPHA= .006
V= 775.9
21-0623
KB3O5
Triklin
Dexp Dcal d(D) h k l
6.4500 6.4494 .0006 -1 0 1
6.0500 6.0499 .0001 -1 1 0
5.8500 5.8520 -.0020 1 -1 2
4.0700 4.0710 -.0010 1 -1 4
3.8400 3.8388 .0012 1 -2 1
3.7700 3.7667 .0033 -2 1 0
3.6900 3.6918 -.0018 -1 2 0
3.5800 3.5799 .0001 -2 0 1
3.5300 3.5288 .0012 0 2 1
3.3800 3.3815 -.0015 0 1 4
3.3400 3.3399 .0001 -1 0 4
3.0800 3.0809 -.0009 2 1 2
A= 8.206 DA= .003
B= 7.8892 DB= .0004
C= 17.46 DC= .01
GAMMA=105.077 DGAMMA= .002
BETA = 74.04 DBETA = .03
ALPHA=103.443 DALPHA= .001
V= 1033.7
21-0624
C8H12BKO8
Triklin
Dexp Dcal d(D) h k l
7.8000 7.7998 .0002 1 1 0
6.9000 6.9033 -.0033 -1 0 1
6.1000 6.1002 -.0002 -1 -2 1
5.4000 5.3993 .0007 0 2 1
4.9000 4.9005 -.0005 0 -3 1
4.2700 4.2710 -.0010 -1 0 2
3.6200 3.6251 -.0051 0 -3 2
3.3700 3.3705 -.0005 -2 2 1
3.0600 3.0604 -.0004 1 2 2
2.9400 2.9391 .0009 -1 -5 2
2.7800 2.7788 .0012 -2 -1 3
2.6600 2.6598 .0002 -2 4 0
A= 8.7008 DA= .0002
B= 16.644 DB= .001
C= 9.034 DC= .002
GAMMA= 77.646 DGAMMA= .003
BETA =107.90 DBETA = .02
ALPHA=102.646 DALPHA= .005
V= 1199.6
21-0625
K4CaH4{P2O7}2
Triklin
Dexp Dcal d(D) h k l
9.7700 9.7707 -.0007 1 0 0
8.5600 8.5540 .0060 0 0 1
5.4800 5.4854 -.0054 0 -2 1
4.5400 4.5405 -.0005 1 -2 1
4.1100 4.1112 -.0012 1 2 1
3.7900 3.7913 -.0013 -1 -3 1
3.5900 3.5864 .0036 2 2 1
3.4600 3.4589 .0011 2 -1 2
3.3100 3.3095 .0005 2 3 0
3.2300 3.2295 .0005 3 0 1
3.1000 3.1013 -.0013 1 3 1
2.9800 2.9794 .0006 -2 0 2
A= 10.1007 DA= .0001
B= 11.7569 DB= .0009
C= 9.1046 DC= .0009
GAMMA= 78.90 DGAMMA= .02
BETA = 84.333 DBETA = .003
ALPHA=107.63 DALPHA= .01
V= 996.8
21-0626
KCaH{P2O7}*2H2O
Triklin
Dexp Dcal d(D) h k l
6.0600 6.0513 .0087 0 1 1
5.6900 5.6908 -.0008 1 0 1
5.0900 5.0929 -.0029 1 1 1
4.8300 4.8234 .0066 0 2 1
4.0600 4.0652 -.0052 1 2 1
3.7000 3.7027 -.0027 0 3 1
3.6300 3.6292 .0008 2 0 1
3.4600 3.4587 .0013 -2 2 0
3.3400 3.3355 .0045 2 1 1
3.2200 3.2149 .0051 1 3 1
3.1600 3.1643 -.0043 2 1 0
3.0500 3.0509 -.0009 0 -3 1
2.9900 2.9923 -.0023 1 2 2
A= 7.6542 DA= .0001
B= 12.3803 DB= .0006
C= 6.6446 DC= .0002
GAMMA=102.0675 DGAMMA= .0003
BETA = 73.030 DBETA = .001
ALPHA= 82.1527 DALPHA= .0001
V=575.7
21-0627
K-Ca-H-P-O
Monoklin
Grupa 4, 11
Dexp Dcal d(D) h k l
9.8200 9.8441 -.0241 0 1 1
5.9400 5.9455 -.0055 -1 1 2
5.8200 5.8212 -.0012 -1 0 3
5.1200 5.1232 -.0032 -1 1 3
4.8700 4.8746 -.0046 1 1 4
4.3900 4.3922 -.0022 0 1 5
4.0700 4.0746 -.0046 2 0 4
3.9000 3.8992 .0008 1 0 6
3.8000 3.8118 -.0118 2 1 4
3.6700 3.6671 .0029 1 1 6
3.5700 3.5697 .0003 2 2 2
3.3200 3.3213 -.0013 -1 3 1
a= 9.8700 b= 10.790 c= 24.2700 beta= 82.153
da= .0001 db= .001 dc=.0001 dbet=.001
V= 2560.5
21-0627
KCa{P2O7}2*4H2O
Triklin
Dexp Dcal d(D) h k l
9.8200 9.8143 .0057 -1 0 1
5.9400 5.9506 -.0106 0 -1 1
5.8200 5.8176 .0024 0 1 2
5.1200 5.1206 -.0006 -2 1 1
4.8700 4.8786 -.0086 1 0 2
4.3900 4.3924 -.0024 2 1 0
4.0700 4.0742 -.0042 -2 1 3
3.9000 3.9009 -.0009 0 2 2
3.8000 3.7971 .0029 -1 2 0
3.6700 3.6703 -.0003 -3 1 2
3.5700 3.5718 -.0018 -1 2 3
3.3200 3.3189 .0011 0 -1 3
A= 11.663 DA= .001
B= 8.380 DB= .004
C= 13.883 DC= .001
GAMMA= 99.29 DGAMMA= .04
BETA =108.90 DBETA = .08
ALPHA= 70.979 DALPHA= .001
V= 1211.4
21-0628
K-Ca-P-H-O
Triklin
Dexp Dcal d(D) h k l
7.3100 7.3142 -.0042 -1 0 1
6.6500 6.6576 -.0076 0 1 1
5.6000 5.5989 .0011 0 -1 1
5.4500 5.4510 -.0010 1 1 1
4.4700 4.4729 -.0029 -2 1 0
3.3300 3.3288 .0012 0 2 2
3.2800 3.2789 .0011 -3 1 0
3.2200 3.2209 -.0009 1 2 1
3.1200 3.1182 .0018 2 -1 3
3.0900 3.0883 .0017 1 1 4
3.0600 3.0623 -.0023 -2 2 1
2.9400 2.9405 -.0005 3 0 3
A= 10.528 DA= .002
B= 7.11067 DB= .00004
C= 13.08 DC= .01
GAMMA= 97.24 DGAMMA= .09
BETA = 80.67 DBETA = .06
ALPHA= 79.69 DALPHA= .05
V= 938.3
21-0629
K2caP2O7*4H2O
Triklin
Dexp Dcal d(D) h k l
10.2000 10.1944 .0056 1 0 1
6.5500 6.5391 .0109 0 1 1
5.0300 5.0280 .0020 1 -1 2
4.8200 4.8196 .0004 2 -1 1
4.6900 4.6916 -.0016 0 -1 2
4.1700 4.1669 .0031 1 0 3
4.0600 4.0602 -.0002 0 2 0
3.8000 3.7982 .0018 0 2 1
3.5200 3.5201 -.0001 2 1 3
3.1800 3.1803 -.0003 2 2 0
3.0900 3.0897 .0003 3 1 3
2.9500 2.9497 .0003 -1 -1 3
A= 11.673 DA= .001
B= 8.127 DB= .002
C= 12.544 DC= .001
GAMMA= 92.07 DGAMMA= .01
BETA = 64.65 DBETA = .04
ALPHA= 91.93 DALPHA= .02
V=1073.9
21-0635
K3Gd4{PO4}5
Triklin
Dexp Dcal d(D) h k l
5.1800 5.1747 .0053 0 1 1
4.4800 4.4784 .0016 0 -1 1
4.0700 4.0749 -.0049 -2 2 0
3.8300 3.8293 .0007 -2 0 1
3.6400 3.6420 -.0020 -1 3 0
3.3200 3.3145 .0055 1 3 0
3.0500 3.0495 .0005 -2 3 1
2.9700 2.9717 -.0017 2 -2 1
2.8410 2.8408 .0002 -2 -2 1
2.6580 2.6586 -.0006 0 4 1
2.5980 2.5983 -.0003 -2 4 0
2.4730 2.4737 -.0007 -4 2 0
A= 10.44287 DA= .00001
B= 11.39272 DB= .00000
C= 5.43315 DC= .00000
GAMMA= 99.43789 DGAMMA= .00002
BETA = 95.70962 DBETA = .00004
ALPHA= 78.66772 DALPHA= .00000
V=623.8
21-0636
KGa5O8
Triklin
Dexp Dcal d(D) h k l
11.8000 11.8013 -.0013 0 1 0
5.9000 5.9007 -.0007 0 2 0
4.8600 4.8607 -.0007 2 2 0
4.4000 4.4004 -.0004 1 1 1
2.9200 2.9199 .0001 -5 1 1
2.8800 2.8803 -.0003 1 4 0
2.7100 2.7095 .0005 4 -3 1
2.6100 2.6101 -.0001 -6 1 1
2.5200 2.5197 .0003 0 -4 1
2.5000 2.5005 -.0005 2 -4 1
2.4300 2.4304 -.0004 4 4 0
2.3400 2.3401 -.0001 -2 5 0
2.2500 2.2495 .0005 2 5 0
A= 19.520 DA= .006
B= 11.845 DB= .001
C= 4.871 DC= .0004
GAMMA= 94.937 DGAMMA= .008
BETA = 87.06 DBETA = .01
ALPHA= 90.106 DALPHA= .009
V=1120.2
21-0637
CH3GeKO2
Triklin
Dexp Dcal d(D) h k l
11.5000 11.5014 -.0014 0 1 0
5.8500 5.8506 -.0006 2 1 0
5.4000 5.4040 -.0040 0 0 1
4.4500 4.4529 -.0029 2 2 0
4.2200 4.2218 -.0018 0 -2 1
3.7000 3.6964 .0036 3 0 1
3.5500 3.5516 -.0016 -2 1 1
3.4000 3.3975 .0025 -3 2 0
3.3400 3.3386 .0014 0 -3 1
3.2000 3.2000 .0000 -1 -3 1
3.0500 3.0511 -.0011 3 2 1
2.9200 2.9215 -.0015 -2 -3 1
A= 13.32 DA= .01
B= 11.608 DB= .002
C= 5.512 DC= .002
GAMMA= 87.95 DGAMMA= .03
BETA = 81.4306 DBETA = .0001
ALPHA= 97.09 DALPHA= .01
V=835.5
21-0638
K2Ge2O5
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.1100 6.1142 -.0042 1 1 0
5.2800 5.2800 .0000 0 0 2
3.1400 3.1397 .0003 -2 0 3
3.0800 3.0797 .0003 0 2 2
2.9000 2.8995 .0005 3 1 1
2.6400 2.6400 .0000 0 0 4
2.2800 2.2799 .0001 0 3 2
2.0100 2.0102 -.0002 1 0 5
1.8300 1.8300 -.0000 -5 2 1
a= 10.4580 b= 7.5830 c= 10.6840 beta= 98.734
da=.0008 db=.0009 dc= .0003 dbet= .003
V= 837.4
21-0640
K6Ge11O25
Rombik
Groupa 17
Dexp. Dcal. d(D) h k l
5.9100 5.9147 -.0047 0 1 0
5.0700 5.0615 .0085 1 1 0
4.9000 4.8912 .0088 2 0 0
3.7700 3.7693 .0007 2 1 0
3.6000 3.6032 -.0032 1 1 2
3.5300 3.5382 -.0082 2 1 1
3.4100 3.4203 -.0103 0 0 3
3.0400 3.0377 .0023 2 1 2
2.9600 2.9574 .0026 0 2 0
2.8600 2.8556 .0044 3 1 0
2.8300 2.8308 -.0008 1 2 0
2.8100 2.8030 .0070 2 0 3
a= 9.782 b= 5.915 c=10.261
da= .003 db= .001 dc= .004
v= 593.7
Monoklin
Grupa 7,13
Dexp Dcal d(D) h k l
5.9100 5.9280 -.0180 0 1 0
5.0700 5.0711 -.0011 0 1 1
4.9000 4.8959 .0041 0 0 2
3.7700 3.7749 -.0049 0 1 2
3.6000 3.6013 -.0013 2 1 1
3.5300 3.5330 -.0030 2 0 2
3.4100 3.4183 -.0083 3 0 0
3.0400 3.0349 .0051 2 1 2
2.9600 2.9612 -.0012 3 1 0
2.8600 2.8592 .0008 0 1 3
2.8300 2.8314 -.0014 3 1 1
2.8100 2.8089 .0011 -2 0 3
a= 10.2550 b= 5.9280 c= 9.7920 beta= 90.253
da= .001 db=.0009 dc=.0002 dbet= .006
V= 595.3
21-0641
KGePO5
Triklin
Dexp Dcal d(D) h k l
6.2400 6.2403 -.0003 1 1 0
5.6900 5.6901 -.0001 1 1 1
5.4000 5.3959 .0041 1 -1 1
4.0800 4.0790 .0010 0 2 0
3.7000 3.6989 .0011 0 -2 1
3.3200 3.3203 -.0003 -1 -2 1
3.0900 3.0878 .0022 -1 1 2
2.9500 2.9501 -.0001 2 -2 1
2.7000 2.7001 -.0001 -3 1 0
2.6600 2.6583 .0017 0 1 3
2.4800 2.4803 -.0003 3 2 0
2.4600 2.4588 .0012 -1 0 3
A= 9.421 DA= .003
B= 8.184 DB= .001
C= 9.028 DC= .001
GAMMA= 85.53 DGAMMA= .04
BETA = 69.98 DBETA = .09
ALPHA= 89.32 DALPHA= .07
V= 652.0
21-0642
KH{SeO3}
Tetragon
Grupa 75
Dexp. Dcal. d(D) h k l
4.8600 4.8800 -.0200 2 1 0
4.8000 4.8029 -.0029 1 1 2
4.0900 4.0911 -.0011 0 0 3
3.6300 3.6374 -.0074 3 0 0
3.3200 3.3219 -.0019 3 1 1
3.1400 3.1351 .0049 2 1 3
3.0200 3.0265 -.0065 3 2 0
2.9400 2.9384 .0016 3 2 1
2.6700 2.6744 -.0044 2 0 4
2.5900 2.5871 .0029 4 1 1
2.0400 2.0387 .0013 4 0 4
a= 10.91 c= 12.27
da= .02 dc= .01
v= 1461
21-0642
KH{SeO3}
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.8600 4.8582 .0018 2 1 0
4.8000 4.7941 .0059 1 2 0
4.0900 4.0947 -.0047 1 0 2
3.6300 3.6285 .0015 2 2 1
3.3200 3.3190 .0010 -2 2 1
3.1400 3.1410 -.0010 -3 0 1
3.0200 3.0209 -.0009 -1 2 2
2.9400 2.9380 .0020 -2 1 2
2.6700 2.6683 .0017 0 4 0
2.5900 2.5920 -.0020 1 4 0
2.0400 2.0399 .0001 5 1 2
a= 11.0678 b= 10.673 c= 8.375 beta= 80.38
da= .0006 db= .009 dc=.009 dbeta=.01
V= 975.5
21-0643
K5H3{SeO3}4
Monoklin
Grupa 4, 11
Dexp Dcal d(D) h k l
4.4300 4.4226 .0074 2 1 0
4.2400 4.2401 -.0001 1 2 0
3.3700 3.3718 -.0018 2 2 1
3.1800 3.1642 .0158 1 0 3
3.1800 3.1806 -.0006 3 1 1
3.1100 3.1108 -.0008 0 0 3
2.8200 2.8215 -.0015 -3 1 1
2.7200 2.7214 -.0014 3 2 0
2.5600 2.5606 -.0006 3 0 3
2.5100 2.5094 .0006 4 0 0
2.3850 2.3851 -.0001 1 0 4
2.2120 2.2113 .0007 4 2 0
1.8380 1.8381 -.0001 5 1 3
1.7920 1.7919 .0001 4 3 3
a= 10.264 b= 9.356 c= 9.5430 beta= 77.932
da=.001 db=.001 dc=.0007 dbet=.007
V= 896.2
21-0644
KH3{SeO3}2
Triklin
Dexp Dcal d(D) h k l
5.8400 5.8429 -.0029 0 0 1
4.3100 4.3101 -.0001 2 0 1
4.0700 4.0687 .0013 0 2 1
3.9300 3.9310 -.0010 -1 2 0
3.4500 3.4507 -.0007 2 2 1
3.1500 3.1493 .0007 -2 2 1
2.8100 2.8113 -.0013 0 3 0
2.7100 2.7102 -.0002 2 -2 1
2.5000 2.5003 -.0003 -2 3 0
2.3280 2.3280 .0000 -1 3 2
2.2740 2.2734 .0006 0 -3 1
2.2490 2.2483 .0007 -4 -1 1
A= 11.280 DA= .002
B= 8.8813 DB= .0007
C= 6.198 DC= .001
GAMMA= 87.03 DGAMMA= .06
BETA = 82.43 DBETA = .04
ALPHA= 71.75 DALPHA= .01
V= 584.6
21-0646
K2B3O3F4OH
Triklin
Dexp Dcal d(D) h k l
4.8400 4.8394 .0006 1 1 0
4.3300 4.3336 -.0036 2 0 0
3.4500 3.4495 .0005 -1 -1 2
3.3700 3.3698 .0002 2 0 3
3.1100 3.1103 -.0003 1 1 4
2.9300 2.9322 -.0022 3 0 1
2.8400 2.8412 -.0012 0 2 0
2.6700 2.6692 .0008 -1 2 0
2.3680 2.3674 .0006 -1 0 5
2.2560 2.2555 .0005 2 2 4
2.1670 2.1668 .0002 4 0 0
2.0820 2.0822 -.0002 -1 -2 3
A= 8.83316 DA= .00005
B= 5.82303 DB= .00003
C= 13.4616 DC= .0003
GAMMA= 85.529 DGAMMA= .001
BETA = 79.103 DBETA = .003
ALPHA= 77.583 DALPHA= .001
V=683.5
21-0649
K3IO5*5H2O
Triklin
Dexp Dcal d(D) h k l
7.9800 7.9808 -.0008 1 1 0
6.7600 6.7644 -.0044 0 1 1
5.5600 5.5601 -.0001 0 -1 1
5.2100 5.2015 .0085 1 2 1
4.9800 4.9808 -.0008 -1 1 0
4.9300 4.9254 .0046 1 2 0
4.6300 4.6296 .0004 1 1 2
4.4600 4.4529 .0071 0 2 0
4.0800 4.0796 .0004 0 1 2
3.9900 3.9904 -.0004 2 2 0
3.6400 3.6414 -.0014 0 -2 1
3.4800 3.4826 -.0026 1 3 1
A= 9.855 DA= .006
B= 10.67 DB= .01
C= 9.291 DC= .002
GAMMA= 58.32 DGAMMA= .04
BETA = 65.71 DBETA = .05
ALPHA= 68.50 DALPHA= .09
V=743.4
21-0651
KLaP2O7
Grupa 4, 11
Dexp Dcal d(D) h k l
4.1500 4.1511 -.0011 -1 1 1
3.5500 3.5522 -.0022 -1 1 3
3.4800 3.4797 .0003 -2 1 2
3.3000 3.2994 .0006 2 1 1
3.0800 3.0799 .0001 0 1 4
2.9980 2.9982 -.0002 1 0 5
2.8670 2.8654 .0016 3 1 0
2.5850 2.5899 -.0049 -4 0 5
2.4280 2.4281 -.0001 -4 1 3
2.3510 2.3510 -.0000 -5 0 2
2.2430 2.2421 .0009 -4 1 5
2.1930 2.1925 .0005 3 0 5
a= 11.7700 b= 4.4790 c= 17.8560 beta= 108.1447
da=.0002 db=.0008 dc=.0001 dbet=.0006
V= 894.5
21-0676
K4P2O7
Triklin
Dexp Dcal d(D) h k l
4.8200 4.8007 .0193 1 1 1
4.6200 4.6188 .0012 0 -1 1
3.5500 3.5506 -.0006 2 2 0
3.4000 3.4010 -.0010 1 3 0
3.2800 3.2763 .0037 1 -2 1
3.0900 3.0903 -.0003 -1 2 1
2.9430 2.9414 .0016 0 3 1
2.9190 2.9183 .0007 -2 -1 1
2.7550 2.7532 .0018 3 1 0
2.7360 2.7368 -.0008 -2 1 1
2.6190 2.6205 -.0015 3 2 0
2.5330 2.5346 -.0016 -1 3 1
A= 8.4942 DA= .0007
B= 10.497 DB= .001
C= 5.4723 DC= .0002
GAMMA= 77.05 DGAMMA= .01
BETA = 76.910 DBETA = .009
ALPHA= 84.15 DALPHA= .01
V=462.5
21-0677
K4P2O7*3H2O
Triklin
Dexp Dcal d(D) h k l
9.2000 9.2100 -.0100 1 0 0
6.7000 6.7085 -.0085 0 -1 1
4.9700 4.9669 .0031 0 0 2
4.7800 4.7898 -.0098 2 0 1
4.5700 4.5708 -.0008 1 -1 2
4.5000 4.5002 -.0002 0 2 0
4.2900 4.2902 -.0002 -2 1 0
3.9300 3.9323 -.0023 2 1 0
3.7700 3.7760 -.0060 1 2 1
3.6200 3.6202 -.0002 -1 1 2
3.4800 3.4828 -.0028 1 0 3
3.2600 3.2581 .0019 1 2 2
A= 9.76524 DA= .00006
B= 9.06289 DB= .00004
C= 10.47282 DC= .00007
GAMMA= 96.7057 DGAMMA= .0002
BETA = 71.5547 DBETA = .0001
ALPHA= 92.7456 DALPHA= .0001
V=873.2
21-0678
KH2P{BH3}2
Rombik
Groupa 34,58
Dexp. Dcal. d(D) h k l
4.9800 4.9800 .0000 2 0 0
4.6000 4.6005 -.0005 1 1 0
3.8600 3.8598 .0002 1 0 1
2.7300 2.7264 .0036 2 1 1
2.5100 2.5098 .0002 1 2 0
a= 9.960 b= 5.187 c= 4.187
da= .001 db= .001 dc= .001
v= 216.3
21-0683
Alfa-K2S2O7
Monoklin
Grupa 14
Dexp Dcal d(D) h k l
4.9300 4.9324 -.0024 -1 1 1
3.4800 3.4802 -.0002 -2 1 1
3.1800 3.1810 -.0010 -1 0 2
3.0400 3.0393 .0007 -1 1 2
2.8100 2.8096 .0004 -2 0 2
2.4800 2.4793 .0007 1 1 2
2.3400 2.3402 -.0002 -1 4 1
2.2200 2.2199 .0001 3 2 0
2.0200 2.0205 -.0005 2 1 2
a= 7.753 b= 10.2960 c= 6.402 beta= 107.815
da=.001 db=.0007 dc=.004 dbet=.003
V= 486.5
21-0692
K2CS3*NH3
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
6.6500 6.6579 -.0079 1 1 0
5.8200 5.8232 -.0032 -1 0 1
4.3700 4.3769 -.0069 0 1 2
3.3900 3.3906 -.0006 0 2 2
3.1200 3.1165 .0035 0 1 3
3.0100 3.0113 -.0013 3 1 0
2.9100 2.9116 -.0016 -2 0 2
2.6960 2.6945 .0015 0 2 3
2.6730 2.6736 -.0006 1 0 4
2.5900 2.5901 -.0001 4 0 2
2.5690 2.5693 -.0003 1 1 4
2.4660 2.4668 -.0008 -2 2 2
2.2740 2.2739 .0001 3 3 2
2.1400 2.1394 .0006 -1 1 4
2.0830 2.0821 .0009 -4 1 1
a= 10.404 b= 9.287 c= 10.813 beta= 66.612
da=.001 db=.001 dc=.0007 dbet=.009
V= 959.0
21-0718
KY{SO4}2*H2O
Triklin
Dexp Dcal d(D) h k l
6.1100 6.1061 .0039 2 1 0
4.1200 4.1132 .0068 0 -3 0
3.7700 3.7693 .0007 2 3 0
3.3600 3.3619 -.0019 2 0 1
3.2200 3.2182 .0018 4 1 0
3.1800 3.1788 .0012 4 0 0
3.0700 3.0685 .0015 0 2 1
3.0300 3.0297 .0003 -2 0 1
2.7520 2.7532 -.0012 1 -3 1
2.6260 2.6262 -.0002 -3 0 1
2.5570 2.5562 .0008 4 1 1
2.4470 2.4463 .0007 0 -4 1
A= 12.995 DA= .002
B= 12.550 DB= .002
C= 3.7077 DC= .0005
GAMMA= 80.25 DGAMMA= .03
BETA = 83.71 DBETA = .05
ALPHA= 92.74 DALPHA= .04
V=590.9
21-0984
KGeH2PO6*H2O
Triklin
Dexp Dcal d(D) h k l
6.3000 6.2836 .0164 0 0 1
3.0100 3.0095 .0005 1 -2 1
2.8900 2.8912 -.0012 0 -2 1
2.7000 2.6995 .0005 0 2 0
2.5100 2.5082 .0018 1 -2 2
2.1600 2.1598 .0002 -2 -1 1
1.9500 1.9497 .0003 2 -3 1
1.8700 1.8699 .0001 -2 2 2
1.7400 1.7411 -.0011 -2 3 1
1.6000 1.6003 -.0003 3 -2 2
1.5300 1.5298 .0002 3 -3 2
1.4800 1.4801 -.0001 0 -3 4
A= 5.845 DA= .003
B= 6.259 DB= .001
C= 6.792 DC= .002
GAMMA=112.16 DGAMMA= .01
BETA = 96.66 DBETA = .01
ALPHA=106.937 DALPHA= .009
V= 212.9
21-0985
KGeH2PO6
Triklin
Dexp Dcal d(D) h k l
7.6500 7.6501 -.0001 1 0 0
5.2600 5.2566 .0034 1 2 0
3.7600 3.7583 .0017 1 2 1
3.5200 3.5181 .0019 2 2 0
2.9500 2.9482 .0018 -1 -2 1
2.6500 2.6493 .0007 0 4 1
1.9600 1.9602 -.0002 2 6 0
1.8700 1.8696 .0004 -1 2 2
1.7200 1.7198 .0002 1 -6 1
1.6600 1.6600 .0000 3 -2 2
1.5700 1.5701 -.0001 2 -4 2
1.5000 1.5003 -.0003 -2 4 2
A= 7.9793 DA= .0007
B= 12.7713 DB= .0005
C= 4.3514 DC= .0002
GAMMA= 79.124 DGAMMA= .008
BETA = 76.183 DBETA = .003
ALPHA= 81.206 DALPHA= .002
V=420.2
21-0986
KGeH2PO6*2H2O
Triklin
Dexp Dcal d(D) h k l
6.3500 6.3457 .0043 1 0 0
5.8400 5.8369 .0031 0 1 1
5.5400 5.5356 .0044 0 -1 1
4.9800 4.9770 .0030 1 1 0
3.7000 3.7001 -.0001 -1 2 1
3.3400 3.3400 .0000 0 3 0
2.9700 2.9669 .0031 -1 1 2
2.8400 2.8409 -.0009 -2 0 1
2.7600 2.7595 .0005 -1 -1 2
2.6900 2.6903 -.0003 -2 2 1
2.6100 2.6112 -.0012 -2 -1 1
2.5100 2.5084 .0016 -1 -3 1
A= 6.45055 DA= .00002
B= 10.194 DB= .003
C= 6.909 DC= .003
GAMMA=100.115 DGAMMA= .007
BETA = 88.334 DBETA = .005
ALPHA= 87.10 DALPHA= .03
V= 446.3
21-0987
KH{PO3F}
Rombik
Groupa 19
romb.
Dexp. Dcal. d(D) h k l
3.7000 3.7034 -.0034 1 1 0
3.4800 3.4775 .0025 1 1 1
3.3700 3.3703 -.0003 0 0 3
3.2300 3.2241 .0059 1 0 3
3.2100 3.2041 .0059 2 1 0
2.9800 2.9800 .0000 3 0 2
a=11.067 b= 3.930 c=10.111
da= .001 db= .001 dc= .001
v= 439.7
21-1290
K{PO2F{NH2}}
Triklin
Dexp Dcal d(D) h k l
5.2100 5.2117 -.0017 1 1 1
4.6700 4.6693 .0007 1 -1 1
4.2700 4.2695 .0005 2 0 0
3.9500 3.9434 .0066 -1 -1 1
3.6400 3.6378 .0022 0 2 1
3.4200 3.4272 -.0072 -1 0 2
3.2300 3.2303 -.0003 1 2 0
3.0900 3.0902 -.0002 0 2 2
2.9500 2.9531 -.0031 -2 -1 1
2.7100 2.7094 .0006 2 -2 1
2.6200 2.6201 -.0001 3 0 2
2.5100 2.5104 -.0004 3 1 2
A= 8.7556 DA= .0001
B= 7.4587 DB= .0001
C= 8.619 DC= .0003
GAMMA= 92.791 DGAMMA= .001
BETA = 78.442 DBETA = .001
ALPHA= 77.762 DALPHA= .001
V=536.5
Triklin
Dexp Dcal d(D) h k l
5.2100 5.2084 .0016 1 3 0
4.6700 4.6673 .0027 0 3 0
4.2700 4.2695 .0005 3 3 0
3.9500 3.9513 -.0013 0 -1 1
3.6400 3.6392 .0008 3 4 0
3.4200 3.4150 .0050 -2 0 1
3.2300 3.2314 -.0014 -3 -2 1
3.0900 3.0913 -.0013 -3 2 0
2.9500 2.9509 -.0009 -3 0 1
2.7100 2.7102 -.0002 3 -1 1
2.6200 2.6187 .0013 -2 4 0
2.5100 2.5108 -.0008 -1 5 0
A= 14.531 DA= .002
B= 15.908 DB= .002
C= 4.0162 DC= .0004
GAMMA= 62.593 DGAMMA= .002
BETA = 95.44 DBETA = .02
ALPHA= 99.12 DALPHA= .01
V=813.4
21-1292
K4H8{P2O7}3
Triklin
Dexp Dcal d(D) h k l
8.8000 8.7889 .0111 1 0 0
6.6000 6.6070 -.0070 -1 1 1
6.3200 6.3080 .0120 -1 -1 1
5.7100 5.7146 -.0046 1 1 1
5.2400 5.2292 .0108 0 0 2
4.4800 4.4805 -.0005 -1 -1 2
4.2400 4.2359 .0041 -1 -2 1
3.9400 3.9416 -.0016 -2 1 2
3.7900 3.7878 .0022 -2 1 0
3.7800 3.7811 -.0011 -1 1 3
3.6900 3.6932 -.0032 2 1 1
3.6300 3.6289 .0011 1 2 2
A= 9.471 DA= .002
B= 10.523 DB= .009
C= 11.521 DC= .002
GAMMA= 84.86 DGAMMA= .02
BETA =109.40 DBETA = .05
ALPHA= 76.97 DALPHA= .05
V=1039.1
21-1300
K3PO4*1.5H2O
Triklin
Dexp Dcal d(D) h k l
6.2200 6.2242 -.0042 -1 1 1
5.3500 5.3536 -.0036 -1 -1 1
5.1700 5.1690 .0010 0 -1 1
4.6600 4.6573 .0027 2 0 0
3.9000 3.9015 -.0015 0 2 0
3.5100 3.5090 .0010 -2 -1 2
3.3800 3.3796 .0004 1 0 2
3.1800 3.1786 .0014 -3 -1 1
3.1300 3.1332 -.0032 -3 1 1
2.9900 2.9927 -.0027 2 -1 1
2.9470 2.9479 -.0009 0 1 3
2.8730 2.8719 .0011 0 0 3
A= 10.3965 DA= .0006
B= 8.066 DB= .001
C= 9.881 DC= .003
GAMMA= 90.25 DGAMMA= .04
BETA =115.68 DBETA = .07
ALPHA= 76.707 DALPHA= .007
V= 722.5
21-1301
K3PO4*7H2O
Triklin
Dexp Dcal d(D) h k l
5.4300 5.4296 .0004 1 0 0
3.6400 3.6399 .0001 -1 1 0
3.3800 3.3828 -.0028 1 -1 2
3.1500 3.1522 -.0022 -1 -1 2
3.0400 3.0362 .0038 0 -1 4
2.7360 2.7356 .0004 2 0 1
2.5610 2.5612 -.0002 2 0 3
2.3810 2.3803 .0007 -2 1 0
2.2200 2.2196 .0004 1 -1 6
2.1300 2.1300 -.0000 -2 0 4
2.0630 2.0628 .0002 1 1 7
2.0210 2.0214 -.0004 0 0 8
A= 5.4754 DA= .0003
B= 4.8680 DB= .0007
C= 16.327 DC= .004
GAMMA= 90.21 DGAMMA= .01
BETA = 82.604 DBETA = .004
ALPHA= 87.24 DALPHA= .04
V= 431.0
21-1302
K3PO4*3H2O
Triklin
Dexp Dcal d(D) h k l
7.3600 7.3587 .0013 1 0 0
6.2100 6.2016 .0084 0 2 0
6.0800 6.0830 -.0030 0 2 2
5.7900 5.7814 .0086 1 1 0
5.4900 5.4919 -.0019 1 1 2
5.3900 5.3787 .0113 -1 2 0
4.7300 4.7298 .0002 1 2 2
4.6700 4.6701 -.0001 0 3 1
4.2300 4.2257 .0043 -1 0 2
4.0100 4.0124 -.0024 -1 3 0
3.7800 3.7828 -.0028 2 0 1
3.7200 3.7197 .0003 -1 2 3
A= 7.64370 DA= .00001
B= 14.33411 DB= .00000
C= 14.15791 DC= .00007
GAMMA= 97.3737 DGAMMA= .0002
BETA = 81.2230 DBETA = .0002
ALPHA= 62.66113 DALPHA= .00004
V=1326.6
21-1645
C18H18K6O21*4H2O
Triklin
Dexp Dcal d(D) h k l
9.6900 9.6907 -.0007 1 0 0
9.3300 9.3333 -.0033 1 1 0
7.6500 7.6463 .0037 -1 -1 2
5.3800 5.3858 -.0058 1 2 0
5.1400 5.1400 -.0000 2 1 1
4.9000 4.8947 .0053 1 2 1
4.6900 4.6908 -.0008 -2 0 1
4.5800 4.5825 -.0025 2 1 2
3.7000 3.7011 -.0011 1 -2 1
3.5200 3.5204 -.0004 3 1 1
3.3000 3.3023 -.0023 0 0 6
3.2700 3.2689 .0011 -2 -3 4
A= 11.0568 DA= .0009
B= 11.133 DB= .001
C= 20.477 DC= .001
GAMMA= 61.233 DGAMMA= .007
BETA = 96.257 DBETA = .008
ALPHA=104.61 DALPHA= .01
V= 2137.9