41-1929
C21H12N3O12Sc*3H2O
Triklin
Dexp Dcal d(D) h k l
13.5480 13.5916 -.0436 1 0 0
11.6970 11.6850 .0120 0 1 0
10.3880 10.4181 -.0301 0 0 1
9.2669 9.2585 .0084 0 1 1
8.1809 8.1867 -.0058 2 1 1
7.5717 7.5917 -.0200 -1 1 0
7.1831 7.2146 -.0315 -1 0 1
6.7914 6.7958 -.0044 2 0 0
6.2611 6.2645 -.0034 1 2 0
6.1920 6.1942 -.0022 1 1 2
5.9308 5.9215 .0093 2 1 2
5.6340 5.6326 .0014 2 2 2
A= 16.73 DA= .02
B= 14.25 DB= .01
C= 12.4946 DC= .0006
GAMMA= 59.20 DGAMMA= .05
BETA = 60.82 DBETA = .05
ALPHA= 61.84 DALPHA= .06
V=2132.3
41-1930
C21H12N3O12Sc*H2O
Triklin
Dexp Dcal d(D) h k l
14.2410 14.2767 -.0357 -1 0 1
10.7910 10.7853 .0057 1 1 0
10.4860 10.4670 .0190 1 0 1
8.5567 8.5734 -.0167 0 -1 1
7.0035 6.9918 .0117 2 0 1
6.6702 6.6697 .0005 -1 -1 2 0
6.2961 6.2912 .0049 -3 0 1
6.1581 6.1670 -.0089 1 1 2
5.3916 5.3926 -.0010 2 2 0
5.2658 5.2640 .0018 2 -1 1
4.9651 4.9656 -.0005 0 1 3
4.8173 4.8178 -.0005 -1 2 0
A= 19.697 DA= .005
B= 11.335 DB= .001
C= 16.71 DC= .01
GAMMA= 73.977 DGAMMA= .008
BETA =106.75 DBETA = .08
ALPHA= 89.33 DALPHA= .06
V=3415.9
41-1931
C21H12N3O12Sc*2H2O
Triklin
Dexp Dcal d(D) h k l
13.0700 13.0827 -.0127 0 1 1
12.2100 12.2022 .0078 0 -1 1
11.0040 10.9986 .0054 1 0 0
10.8960 10.8923 .0037 1 0 1
8.3646 8.3786 -.0140 0 1 2
7.9483 7.9391 .0092 -1 1 1
7.5208 7.5245 -.0037 1 -1 2
6.5919 6.6020 -.0101 1 2 1
6.5153 6.5019 .0134 1 2 0
6.1581 6.1509 .0072 1 0 3
5.6909 5.6929 -.0020 -1 -1 2
5.5782 5.5764 .0018 2 -1 1
A= 11.503 DA= .005
B= 17.42 DB= .01
C= 19.22 DC= .02
GAMMA= 94.70 DGAMMA= .05
BETA = 73.91 DBETA = .02
ALPHA= 87.48 DALPHA= .03
V= 3679.5