36-0669
Sc{TcO4}3*H2O
Triklin
Dexp Dcal d(D) h k l
5.4700 5.4726 -.0026 -1 1 0
3.5600 3.5590 .0010 -1 1 1
2.9200 2.9194 .0006 -1 -1 1
2.5600 2.5607 -.0007 -2 1 1
2.2000 2.1999 .0001 -2 3 0
2.0700 2.0696 .0004 -1 0 2
1.9600 1.9596 .0004 0 4 1
1.8700 1.8699 .0001 -1 3 2
1.7600 1.7602 -.0002 2 -2 2
1.6100 1.6104 -.0004 -2 -3 1
1.5700 1.5705 -.0005 -1 5 1
1.5300 1.5305 -.0005 -1 -4 1
A= 6.906 DA= .001
B= 7.996 DB= .001
C= 4.860 DC= .002
GAMMA= 95.62 DGAMMA= .02
BETA = 80.06 DBETA = .02
ALPHA= 77.08 DALPHA= .01
V= 255.0
36-0670
Sc{TcO4}3
Triklin
Dexp Dcal d(D) h k l
3.5700 3.5708 -.0008 0 0 2
3.1500 3.1490 .0010 0 -2 2
2.4100 2.4092 .0008 2 2 0
2.2700 2.2703 -.0003 -1 1 2
2.1500 2.1502 -.0002 2 0 2
2.0900 2.0902 -.0002 -2 -2 2
1.9300 1.9301 -.0001 0 -4 2
1.8700 1.8700 -.0000 0 -2 4
1.7900 1.7912 -.0012 -1 1 3
1.7500 1.7500 -.0000 0 -3 4
1.7000 1.6988 .0012 -1 -3 4
1.6000 1.5995 .0005 -3 -3 1
A= 5.149 DA= .002
B= 8.197 DB= .003
C= 7.575 DC= .003
GAMMA= 73.78 DGAMMA= .04
BETA = 88.51 DBETA = .01
ALPHA=108.18 DALPHA= .04
V= 289.4
36-1504
C8H5O5Sc*H2O
Triklin
Dexp Dcal d(D) h k l
12.2770 12.2722 .0048 1 0 0
7.3143 7.3181 -.0038 0 1 2
6.4635 6.4588 .0047 0 2 0
5.9061 5.9076 -.0015 -1 2 1
5.4712 5.4687 .0025 1 2 1
5.2155 5.2173 -.0018 0 0 3
4.8742 4.8743 -.0001 2 1 2
4.6465 4.6470 -.0005 1 -2 2
4.4838 4.4827 .0011 0 2 3
4.1141 4.1168 -.0027 2 2 0
3.9689 3.9687 .0002 0 -3 1
3.8176 3.8173 .0003 1 3 2
A= 12.5932 DA= .0004
B= 13.2732 DB= .0002
C= 16.1096 DC= .0002
GAMMA= 98.044 DGAMMA= .001
BETA = 81.3265 DBETA = .0009
ALPHA= 80.835 DALPHA= .003
V=2590.5
36-1505
C16H13Sc3*1.5H2O
Geksagon
Groupa 186,190,194
Dexp. Dcal. d(D) h k l
7.7618 7.7651 -.0033 1 0 1
6.0670 6.0533 .0137 2 1 0
5.0108 5.0015 .0093 2 1 1
4.6226 4.6233 -.0007 2 2 0
3.6776 3.6742 .0034 3 2 0
2.9593 2.9595 -.0002 0 0 3
2.5636 2.5645 -.0009 5 2 0
a= 18.49 c= 8.88
da= .02 dc=.01
v=2629
36-1506
C-H-O-Sc
Triklin
Dexp Dcal d(D) h k l
9.5090 9.5105 -.0015 0 1 1
8.0431 8.0311 .0120 0 -1 1
5.7167 5.7291 -.0124 -1 1 0
5.6803 5.6861 -.0058 1 0 1
5.2155 5.2229 -.0074 1 -1 1
4.8478 4.8421 .0057 0 -2 1
4.5754 4.5683 .0071 -1 1 2
4.5521 4.5515 .0006 -1 -1 1
4.4394 4.4461 -.0067 -1 2 0
4.3533 4.3521 .0012 1 -1 2
3.7385 3.7383 .0002 -1 1 3
3.5065 3.5069 -.0004 0 3 2
A= 6.171 DA= .006
B= 11.277 DB= .001
C= 14.400 DC= .006
GAMMA= 98.95 DGAMMA= .06
BETA = 89.09 DBETA = .01
ALPHA= 80.311 DALPHA= .007
V= 974.8
36-1507
C9H3O6Sc*6H2O
Triklin
Dexp Dcal d(D) h k l
11.1910 11.1895 .0015 1 0 0
6.8099 6.8109 -.0010 1 0 1
5.3085 5.3090 -.0005 -1 -2 1
5.0965 5.0975 -.0010 1 2 0
4.5521 4.5526 -.0005 1 -1 2
4.2503 4.2484 .0019 -1 0 3
3.6627 3.6623 .0004 -3 -1 1
3.5065 3.5076 -.0011 2 -1 2
3.1978 3.1981 -.0003 -3 2 3
3.0893 3.0904 -.0011 -4 1 1
2.8488 2.8491 -.0003 -3 4 1
2.7467 2.7464 .0003 -4 3 2
A= 12.5038 DA= .0003
B= 13.418 DB= .009
C= 12.798 DC= .004
GAMMA=101.64 DGAMMA= .03
BETA =112.62 DBETA = .01
ALPHA= 93.66 DALPHA= .01
V= 1917.5
36-1508
C9H3O6Sc*8H2O
Triklin
Dexp Dcal d(D) h k l
8.5881 8.5859 .0022 1 1 0
8.1167 8.1189 -.0022 -1 1 1
7.0811 7.0809 .0002 -1 -1 1
6.4168 6.4181 -.0013 1 2 0
6.2370 6.2422 -.0052 -1 2 0
4.9829 4.9825 .0004 1 2 1
4.7450 4.7436 .0014 -1 3 0
4.4615 4.4616 -.0001 0 0 2
3.7385 3.7385 .0000 2 1 1
3.4663 3.4662 .0001 -3 -1 1
3.2090 3.2091 -.0001 2 4 0
2.7063 2.7063 .0000 -3 3 3
A= 10.7727 DA= .0004
B= 16.840 DB= .005
C= 9.919 DC= .001
GAMMA= 93.2373 DGAMMA= .0008
BETA =113.326 DBETA = .004
ALPHA= 78.089 DALPHA= .003
V= 1616.2
36-1952
C21H12N3O12Sc*0.5H2O
Triklin
Dexp Dcal d(D) h k l
11.0510 11.0396 .0114 2 0 0
9.3090 9.2964 .0126 -2 1 0
8.8451 8.8492 -.0041 -1 0 1
8.4250 8.4372 -.0122 1 0 1
7.1958 7.1972 -.0014 0 2 0
6.8624 6.8847 -.0223 -3 1 0
6.3709 6.3771 -.0062 -2 2 0
6.2370 6.2648 -.0278 3 1 0
5.9855 5.9865 -.0010 -3 0 1
5.8288 5.8298 -.0010 -3 1 1
5.4712 5.4730 -.0018 -3 2 0
5.3085 5.3085 .0000 3 -1 1
A= 22.29 DA= .01
B= 14.543 DB= .005
C= 9.437 DC= .001
GAMMA= 96.99 DGAMMA= .08
BETA = 94.34 DBETA = .02
ALPHA= 85.20 DALPHA= .02
V=3023
36-1953
C14H10Cl2O7Sc2*H2O
Triklin
Dexp Dcal d(D) h k l
10.7820 10.7791 .0029 1 0 0
7.6284 7.6363 -.0079 -1 1 0
6.6569 6.6580 -.0011 -1 0 1
5.6803 5.6791 .0012 0 0 2
5.3724 5.3710 .0014 0 -1 2
5.0676 5.0696 -.0020 1 1 2
4.7703 4.7713 -.0010 0 2 1
4.0221 4.0210 .0011 1 -1 3
3.9002 3.8969 .0033 -2 1 1
3.7385 3.7401 -.0016 0 2 2
3.5617 3.5621 -.0004 2 2 2
3.3759 3.3765 -.0006 1 -3 2
A= 11.6531 DA= .0001
B= 11.312 DB= .002
C= 12.389 DC= .001
GAMMA= 91.0861 DGAMMA= .0008
BETA = 67.757 DBETA = .009
ALPHA= 97.705 DALPHA= .003
V= 1497.0
39-1954
C28H20O13Sc2*3H2O
Triklin
Dexp Dcal d(D) h k l
11.7870 11.7969 -.0099 2 0 0
10.9150 10.9245 -.0095 1 1 0
10.0480 10.0977 -.0497 0 -1 1
9.1180 9.0678 .0502 -1 -1 1
8.9340 8.9171 .0169 1 1 1
8.7577 8.7791 -.0214 0 1 1
8.5058 8.4734 .0324 -2 0 1
7.8999 7.8986 .0013 3 0 1
7.0586 7.0612 -.0026 1 -1 2
6.6569 6.6581 -.0012 3 1 1
6.4635 6.4652 -.0017 -1 -1 2
6.1936 6.1989 -.0053 -3 1 0
A= 24.489 DA= .002
B= 11.7854 DB= .0007
C= 16.504 DC= .002
GAMMA= 85.52 DGAMMA= .01
BETA = 75.83 DBETA = .03
ALPHA= 97.00 DALPHA= .02
V=4554.1
36-1955
C21H18N3O6Sc
Triklin
Dexp Dcal d(D) h k l
11.0510 11.0542 -.0032 -1 0 1
9.2130 9.2310 -.0180 1 0 1
8.1916 8.2026 -.0110 0 0 2
7.2546 7.2558 -.0012 0 -1 1
6.8624 6.8570 .0054 -1 1 2
6.4168 6.4129 .0039 -1 -1 1
5.6088 5.6281 -.0193 -2 1 1
5.4712 5.4684 .0028 0 0 3
5.3403 5.3470 -.0067 -2 1 0
5.0965 5.1037 -.0072 2 1 0
4.5754 4.5758 -.0004 -2 0 3
4.3323 4.3318 .0005 -2 -1 2
A= 12.9483 DA= .0006
B= 9.654 DB= .002
C= 17.414 DC= .001
GAMMA= 96.063 DGAMMA= .001
BETA =101.8834 DBETA = .0003
ALPHA= 73.440 DALPHA= .005
V=2040.9