49-2149
C144H264N24O24Cr2N12O6S12U3
Triklin
Dexp Dcal d(D) h k l
11.9100 11.8982 .0118 1 0 0
10.5400 10.5458 -.0058 -1 1 0
10.3600 10.3639 -.0039 1 0 1
9.3800 9.3885 -.0085 0 2 0
8.3800 8.3891 -.0091 0 0 2
7.6800 7.6581 .0219 0 2 2
7.2300 7.2266 .0034 0 -2 1
6.8100 6.8103 -.0003 -1 1 2
6.6400 6.6370 .0030 0 3 1
6.4700 6.4705 -.0005 -1 0 2
6.0800 6.0879 -.0079 0 3 2
5.9400 5.9396 .0004 -1 3 1
A= 12.02 DA= .01
B= 19.966 DB= .004
C= 17.90 DC= .01
GAMMA= 93.56 DGAMMA= .09
BETA = 84.11 DBETA = .05
ALPHA= 70.97 DALPHA= .01
V= 4022
49-2151
C24H16N2O4U
Rombik
Groupa 26,28,51
Dexp. Dcal. d(D) h k l
4.6837 4.6807 .0030 0 3 0
3.8289 3.8309 -.0020 1 0 1
2.8278 2.8283 -.0005 1 0 3
2.5890 2.5882 .0008 1 4 1
2.0036 2.0032 .0004 2 1 0
1.9174 1.9173 .0001 1 6 2
1.7225 1.7225 .0000 0 4 6
1.5308 1.5309 -.0001 2 6 0
1.4822 1.4823 -.0001 2 6 2
a= 4.0478 b=14.042 c=11.860
da= .000287 db= .001458 dc= .003525
V= 674.2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
4.6837 4.6834 .0003 1 1 0
3.8289 3.8285 .0004 -1 1 2
2.8278 2.8280 -.0002 0 0 4
2.5890 2.5893 -.0003 -2 0 4
2.0036 2.0036 .0000 2 1 4
1.9174 1.9174 .0000 3 1 3
1.7225 1.7225 -.0000 2 3 0
1.5308 1.5308 .0000 5 1 1
1.4822 1.4822 .0000 -3 1 7
a=8.4330 b= 5.686 c= 11.5490 beta= 101.621
da=.0002 db=.001 dc=.0007 dbeta=.003
V= 542.4
Triklin
Dexp Dcal d(D) h k l
4.6837 4.6839 -.0002 -1 1 0
3.8289 3.8289 .0000 0 -1 1
2.8278 2.8278 .0000 1 -1 2
2.5890 2.5890 -.0000 1 1 2
2.0036 2.0036 .0000 2 -2 2
1.9174 1.9174 .0000 -1 1 3
1.7225 1.7225 .0000 -1 2 3
1.5308 1.5308 .0000 -3 1 2
1.4822 1.4822 .0000 1 3 0
A= 5.94092 DA= .00001
B= 5.53423 DB= .00001
C= 6.79515 DC= .00001
GAMMA=110.6614 DGAMMA= .0001
BETA = 77.6836 DBETA = .0002
ALPHA= 87.84620 DALPHA= .00001
V= 202.67
49-2152
C26H20N2O6U
geksagon.
Groupa 169,170,179
Dexp. Dcal. d(D) h k l
3.2285 3.2254 .0031 2 1 1
2.4017 2.4014 .0003 4 0 1
1.9953 1.9972 -.0019 5 0 1
1.8056 1.8041 .0015 3 2 2
1.5308 1.5300 .0008 2 2 3
1.4449 1.4449 -.0000 5 2 2
1.2884 1.2888 -.0004 1 1 4
1.2236 1.2236 -.0000 5 4 2
a= 12.461 c= 5.269
da=.004 dc=.008
v= 708.5
Monoklin
Grupa 4,11
Dexp Dcal d(D) h k l
3.2285 3.2286 -.0001 2 0 1
2.4017 2.4015 .0002 -1 1 1
1.9953 1.9954 -.0001 4 1 0
1.8056 1.8058 -.0002 -4 1 1
1.5308 1.5307 .0001 0 2 0
1.4449 1.4450 -.0001 -4 1 2
1.2884 1.2884 .0000 -7 1 1
1.2236 1.2236 .0000 -1 2 2
a= 10.525 b= 3.061435 c=4.1391 beta= 90.89
da= 3.811 db=.000007 dc=.0002 dbeta=.0002
V= 133.36
49-2247
С10H10N2*UO2F2
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.2700 10.2594 .0106 0 1 0
9.6200 9.6136 .0064 0 1 1
6.3700 6.3701 -.0001 1 1 2
5.6600 5.6580 .0020 2 0 0
4.6700 4.6721 -.0021 1 2 0
4.2800 4.2796 .0004 -1 2 3
3.5800 3.5801 -.0001 -3 1 1
3.4200 3.4200 .0000 0 2 6
3.0800 3.0800 -.0000 -1 0 9
a=11.464 b=10.259 c= 27.89 beta=99.21
da=.005 db= .001 dc=.01 dbeta=.03
V= 3238
49-2248
C2.9H4N0.7*UO2F2{OH}0.5
Monoklin
Grupa 3
Dexp Dcal d(D) h k l
10.1100 10.1362 -.0262 2 0 0
9.1700 9.1737 -.0037 -2 0 1
6.2100 6.2114 -.0014 0 0 2
4.6400 4.6428 -.0028 1 1 0
4.3000 4.3004 -.0004 4 0 1
3.5800 3.5774 .0026 5 0 1
3.3800 3.3799 .0001 -6 0 2
3.0900 3.0895 .0005 3 1 2
2.3600 2.3601 -.0001 8 0 1
a= 21.07 b=4.77 c= 12.9 beta= 105.82
da=.03 db=.01 dc=.1 dbeta=.04
V= 1248
Triklin
Dexp. Dcal. d(D) h k l
10.1100 10.1100 .0000 0 1 0
9.1700 9.1700 .0000 1 1 0
6.2100 6.1994 .0106 2 1 0
4.6400 4.6403 -.0003 0 1 1
4.3000 4.3000 .0000 3 0 0
3.5800 3.5795 .0005 -2 1 1
3.3800 3.3805 -.0005 -1 2 1
3.0900 3.0883 .0017 3 2 1
2.3600 2.3585 .0015 5 3 0
A= 13.3393 DA= .0006
B= 10.4678 DB= .0008
C= 5.09422 DC= .0002
GAMMA= 75.26 DGAMMA= .01
BETA = 89.4 DBETA = .02
ALPHA= 87.09 DALPHA= .04
V= 687